Movie S2.

TIRF imaging of hydrogen evolution reaction on gold nanoplates supported on an ITO electrode during a voltage scan at 100 mV/s from +0.5 to -1.8 V vs Pt QRE in water containing 25 mM H2SO4, 1 M Na2SO4, and 5 nM R6G. Video was recorded at 19.81 frames/s with a 50-ms exposure time and played in real time. Scale bar is 5 μm.

Imaging nanobubble nucleation and hydrogen spillover during electrocatalytic water splitting

Rui Hao, Yunshan Fan, Marco D. Howard, Joshua C. Vaughan, and Bo Zhang

PNAS. 2018. 115:5878-5883 DOI: 10.1073/pnas.1800945115